Laboratory Techniques in Pharmacy

Teaching Methodologies

Theoretical Matrix:
Essentially expository methodology by appropriate audiovisual media, calling for student participation.
Practice Matrix:
Dividing the class into groups of 2-3 students for practical laboratory.
Continuous evaluation:
Two written Theoretical Tests and two Experimental Works during classes.
Students must obtain a positive rating (10-20) in both matrices (T and P) and cannot have any rating lower than 8 values.
The presence, punctuality, and participation of students in classes is valued in the final calculation of the continuous assessment.
The calculation of the final grade results in 90% of the arithmetic mean of the ratings of both matrices (T and P) and 10% of the attendance assessment.
Regular period Exam, Appeal period Exam and Special period Exam, in accordance with the Academic Regulation in force.

Learning Results

i) Acquisition of theoretical bases to support laboratory work in the field of Chemistry and Pharmacy
ii) Acquisition of basic skills for laboratory work in the areas of Chemistry and Pharmacy, complying with the appropriate safety and quality rules.
iii) Development of autonomy at the laboratory.

Program

T
Safety standards in Laboratory
Material and equipment
Determination of mass,volume and temperature
Density
Pharmaceutical Operations Proper:
Operations of Mechanical Separation of solids:Triage,Sieving
Operations of Separating solids from liquids or immiscible liquids:Decantation,centrifugation
Filtration,Clarification
Operations of Division of Solids:Coarse Division, pulverization
Mass Transfer Operations:Leaching
drying of solids: freeze-drying
primary substance.Primary and secondary standard
Types, classification and concentration units of solutions
Sterilization:Concept,Physical and Chemical methods
P
Medical papers
determination of density
Alcohol at several degrees
Preparation of macerates, decoctions and infusions for later use in syrups and solutions for external use
Preparation of aqueous and alcoholic solutions
Pulverization, sieving and powder mixing
Preparation of composite powders and packaging in medical papers
Preparation of a standard solution and measurement of a solution of unknown concentration

Internship(s)

NAO

Bibliography

Nogueira Prista, L., Correia Alves, A., Morgado, R., Sousa Lobo, J., Tecnologia Farmacêutica, I e II vols, 8ª Edição, Fundação Calouste Gulbenkian. Lisboa 2011

Pombeiro A. J. L. O., Técnicas e Operações Unitárias em Química Laboratorial, 4ª Edição, Fundação Calouste Gulbenkian. Lisboa 2003.